ASTM D7968-17a
采用液相色譜串聯(lián)質(zhì)譜法(LC/MS/MS)測定土壤中多氟化合物的標(biāo)準(zhǔn)試驗方法
Standard Test Method for Determination of Polyfluorinated Compounds in Soil by Liquid Chromatography Tandem Mass Spectrometry (LC/MS/MS)
- 標(biāo)準(zhǔn)號
- ASTM D7968-17a
- 發(fā)布
- 2017年
- 總頁數(shù)
- 24頁
- 發(fā)布單位
- 美國材料與試驗協(xié)會
- 替代標(biāo)準(zhǔn)
- ASTM D7968-23
- 當(dāng)前最新
- ASTM D7968-23
- 引用標(biāo)準(zhǔn)
- ASTM D1193 ASTM D2777 ASTM D5847 ASTM E2554
- 適用范圍
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5.1 This test method has been developed by the U.S. EPA Region 5 Chicago Regional Laboratory (CRL).
5.2 PFCs are widely used in various industrial and commercial products; they are persistent, bio-accumulative, and ubiquitous in the environment. PFCs have been reported to exhibit developmental toxicity, hepatotoxicity, immunotoxicity, and hormone disturbance. A draft Toxicological Profile for Perfluoroalkyls from the U.S. Department of Health and Human Services is available.7 PFCs have been detected in soils, sludges, and surface and drinking waters. Hence, there is a need for a quick, easy, and robust method to determine these compounds at trace levels in various soil matrices for understanding of the sources and pathways of exposure.
5.3 This method has been used to determine selected polyfluorinated compounds in sand (Table 4) and four ASTM reference soils (Table 5).
TABLE 4 Single-Laboratory Recovery Data in Ottawa Sand